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261883

C=CCc1cc(C=C2SC(=S)NC2=O)cc(CC=C)c1O

5-[(3,5-di-2-propenyl-4-hydroxyphenyl)-methylene]-2-thioxo-4-thiazolidinone

Ausbeute 94.6%DOI: 10.6084/m9.figshare.5104873.v1

CCOC(=S)CC/C(C)=C/Cc1c(OC)c(C)c2c(c1OC(N)=O)C(=O)OC2

ethyl (E)-6-(1,3-dihydro-4-carbamoyl oxy-6-methoxy-7-methyl-3-oxo-5-iso benzofuranyl)-4-methyl-4-thiohexenoate

DOI: 10.6084/m9.figshare.5104873.v1

CCOC(=S)CC/C(C)=C/Cc1c(OC)c(C)c2c(c1OC(C)=O)C(=O)OC2

ethyl (E)-6-(1,3-dihydro-4-acetoxy-6-methoxy-7-methyl-3-oxo-5-isobenzofuranyl)-4-methyl-4-thiohexenoate

DOI: 10.6084/m9.figshare.5104873.v1

$COc1c(C)c2c(c(O)c1C/C=C(\C)CCC(=O)Cl)C(=O)OC2$

E-6-(1,3-dihydro-4-hydroxy-6-methoxy-7-methyl-3-oxo-5-isobenzofuranyl)-4-methyl-4-hexenoic acid chloride

DOI: 10.6084/m9.figshare.5104873.v1

$COc1c(C)c2c(c(OC(=O)C34CC5CC(CC(C5)C3)C4)c1C/C=C(\C)CCC(=O)OCCN1CCOCC1)C(=O)OC2$

morpholinoethyl E-6-[1,3-dihydro-4-(1-adamantoyloxy)-6-methoxy-7-methyl-3-oxo-5-isobenzofuranyl]-4-methyl-4-hexenoate

DOI: 10.6084/m9.figshare.5104873.v1

$COc1c(C)c2c(c(OC(N)=O)c1C/C=C(\C)CCC(=O)OCCN1CCOCC1)C(=O)OC2$

morpholinoethyl E-6-(1,3-dihydro-4-carbamoyloxy-6-methoxy-7-methyl-3-oxo-5-isobenzofuranyl)-4-methyl-4-hexenoate

DOI: 10.6084/m9.figshare.5104873.v1

C=CCc1cc(C(=O)OC)cc(CC=C)c1O

Ausbeute 97.0%DOI: 10.6084/m9.figshare.5104873.v1

C=CCc1cc(C(=O)OC)cc(CC=C)c1O[Si](C)(C)C(C)(C)C

Ausbeute 97.2%DOI: 10.6084/m9.figshare.5104873.v1

CCCc1cc(C(=O)OC)cc(CCC)c1O[Si](C)(C)C(C)(C)C

Ausbeute 90.0%DOI: 10.6084/m9.figshare.5104873.v1

COc1c(C)c2c(c(O)c1CC=C(C)COCP(=O)(OC(C)C)OC(C)C)C(=O)OC2

Reaction #61225

[4-(4-hydroxy-6-methoxy-7-methyl-3-oxo-1,3-dihydro-isobenzofuran-5-yl)-2-methyl-but-2-enyloxymethyl]-phosphonic acid diisopropyl ester

Ausbeute 32.0%DOI: 10.6084/m9.figshare.5104873.v1

COc1c(C)c2c(c(O)c1CC=C(C)C=CP(=O)(O)O)C(=O)OC2

Reaction #61226

[5-(4-Hydroxy-6-methoxy-7-methyl-3-oxo-1,3-dihydro-isobenzofuran-5-yl)-3-methyl-penta-1,3-dienyl]-phosphonic acid

DOI: 10.6084/m9.figshare.5104873.v1

COc1c(C)c2c(c(O)c1CC=C(C)CBr)C(=O)OC2

Reaction #61227

6-(4-bromo-3-methyl-but-2-enyl)-7-hydroxy-5-methoxy-4-methyl-3H-isobenzofuran-1-one

Ausbeute 42.3%DOI: 10.6084/m9.figshare.5104873.v1

CCOP(=O)(CCC(C)=CCc1c(O)c2c(c(C)c1OC)COC2=O)OCC

Reaction #61228

[5-(4-hydroxy-6-methoxy-7-methyl-3-oxo-1,3-dihydro-isobenzofuran-5-yl)-3-methyl-pent-3-enyl]-phosphonic acid diethyl ester

DOI: 10.6084/m9.figshare.5104873.v1

CCOP(=O)(O)CCC(C)=CCc1c(O)c2c(c(C)c1OC)COC2=O

Reaction #61229

[5-(4-hydroxy-6-methoxy-7-methyl-3-oxo-1,3-dihydro-isobenzofuran-5-yl)-3-methyl-pent-3-enyl]-phosphonic acid monoethyl ester

Ausbeute 28.0%DOI: 10.6084/m9.figshare.5104873.v1

COC(=O)C(CC=CCBr)CC(C)=CCc1c(O)c2c(c(C)c1OC)COC2=O

Reaction #61230

2-(4-bromo-but-2-enyl)-6-(4-hydroxy-6-methoxy-7-methyl-3-oxo-1,3-dihydro-isobenzofuran-5-yl)-4-methyl-hex-4-enoic acid methyl ester

Ausbeute 78.3%DOI: 10.6084/m9.figshare.5104873.v1

CCOP(=O)(CC=CCC(CC(C)=CCc1c(O)c2c(c(C)c1OC)COC2=O)C(=O)OC)OCC

Reaction #61231

2-[4-(diethoxy-phosphoryl)-but-2-enyl]-6-(4-hydroxy-6-methoxy-7-methyl-3-oxo-1,3-dihydro-isobenzofuran-5-yl)-4-methyl-hex-4-enoic acid methyl ester

Ausbeute 44.5%DOI: 10.6084/m9.figshare.5104873.v1

CCOP(=O)(CC=CCC(CC(C)=CCc1c(O)c2c(c(C)c1OC)COC2=O)C(=O)O)OCC

Reaction #61232

2-[4-(diethoxy-phosphoryl)-but-2-enyl]-6-(4-hydroxy-6-methoxy-7-methyl-3-oxo-1,3-dihydro-isobenzofuran-5-yl)-4-methyl-hex-4-enoic acid

Ausbeute 100.0%DOI: 10.6084/m9.figshare.5104873.v1

CCOP(=O)(O)CC=CCC(CC(C)=CCc1c(O)c2c(c(C)c1OC)COC2=O)C(=O)O

Reaction #61233

2-[4-(ethoxy-hydroxy-phosphoryl)-but-2-enyl]-6-(4-hydroxy-6-methoxy-7-methyl-3-oxo-1,3-dihydro-isobenzofuran-5-yl)-4-methyl-hex-4-enoic acid

Ausbeute 89.0%DOI: 10.6084/m9.figshare.5104873.v1

COC(=O)C(CC=CCP(=O)(OC)OC)CC(C)=CCc1c(O)c2c(c(C)c1OC)COC2=O

Reaction #61234

Ausbeute 88.2%DOI: 10.6084/m9.figshare.5104873.v1

COc1c(C)c2c(c(O)c1CC=C(C)CC(CC=CCP(=O)(OC)OC)C(=O)O)C(=O)OC2

Reaction #61235

desired product

DOI: 10.6084/m9.figshare.5104873.v1

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