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COc1ccc2c(c1)CCC1(C#N)C2=CCC2(C)C(OC3CCCCO3)CCC12
Reaction #230123
DOI: 10.1039/C8SC04228D
COc1ccc2c(c1)CCC1(C)C2CCC2(C)C(O)CCC21
Reaction #1628690
DOI: 10.1039/C8SC04228D
COc1ccc2c(c1)CC[C@]1(C#N)C2=C(CCCCCOCc2ccccc2)C[C@]2(C)[C@@H](OC3CCCCO3)CC[C@H]21
Reaction #2310516
colorless foam 4
Ausbeute 100.2%DOI: 10.6084/m9.figshare.5104873.v1
COc1ccc2c(c1)CC[C@]1(C=O)C2=C(CCCCCOCc2ccccc2)C[C@]2(C)[C@@H](O[Si](C)(C)C(C)(C)C)CC[C@H]21
Reaction #2310517
silyl ether
Ausbeute 93.2%DOI: 10.6084/m9.figshare.5104873.v1
COc1ccc2c(c1)CC[C@@]1(C=O)[C@@H]3CC[C@H](O[Si](C)(C)C(C)(C)C)[C@@]3(C)C[C@H](CCCCCO)[C@H]21
Reaction #2310518
7
Ausbeute 67.3%DOI: 10.6084/m9.figshare.5104873.v1
COc1ccc2c(c1)CC[C@]1(C#N)C2=CC[C@]2(C)[C@@H](OC3CCCCO3)CC[C@H]21
Reaction #2311226
8-cyano-3-methoxy-17β-(tetrahydropyran-2-yloxy)-estra-1,3,5(10),9(11)-tetraene
DOI: 10.6084/m9.figshare.5104873.v1
COc1ccc2c(c1)CC[C@@]1(C)[C@@H]3CC[C@H](O)[C@@]3(C)CC[C@H]21
Reaction #2311227
3-methoxy-8β-methyl-estra-1,3,5(10)-trien-17β-ol
DOI: 10.6084/m9.figshare.5104873.v1
C[C@]12CC=C3c4ccc(O)cc4CC[C@@]3(C=C(F)F)[C@@H]1CC[C@@H]2O
Reaction #2311229
8β-(2,2-difluorovinyl)-estra-1,3,5(10),9(11)-tetraene-3,17β-diol
DOI: 10.6084/m9.figshare.5104873.v1
COc1ccc2c(c1)CCC1(C=O)C2=C(CCCCCOCc2ccccc2)CC2(C)C(O[Si](C)(C)C(C)(C)C)CCC12
Reaction #2397610
DOI: 10.1039/C8SC04228D