反应 #994

反应方程式

2-Methoxy-cinnamylalcohol

thionylchloride

piperazine

→

salt

N,N'-bis-((E)-3-(2-methoxyphenyl)-2-propenyl)piperazine

反应条件

后处理

1. 1
   其他as described in Preparation Example 2

实验过程

2-Methoxy-cinnamylalcohol (1.44 g) was chlorinated using thionylchloride. Subsequently, reaction with piperazine and other treatments were performed as described in Preparation Example 2, to thereby obtain 314 mg of a salt as colorless prisms.

来源