反应 #992686

反应方程式

3,5-Diamino-1,2,4-triazole

Trifluoroacetic acid

→

3,5-Diamino-1,2,4-Triazolium TFA

溶剂

water

反应条件

后处理

1. 1
   其他The water was removed in vacuo
2. 2
   温度with heating to approximately 90° C. for 4 hours

实验过程

3,5-Diamino-1,2,4-triazole (1.50 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

来源