反应 #992679

反应方程式

Hydrazine monohydrate

Trifluoroacetic acid

→

Hydrazinium TFA

溶剂

water

反应条件

后处理

1. 1
   workup.STIRRINGthe reaction was stirred at room temperature overnight
2. 2
   其他The water was removed in vacuo
3. 3
   温度with heating to 80° C.
4. 4
   其他yielding product as a colorless liquid

实验过程

Hydrazine monohydrate (4.41 ml, 90.9 mmol) was added via syringe to a 250-ml round-bottom flask containing 50 ml of distilled water with stirring at room temperature. Trifluoroacetic acid (7.0 ml, 90.9 mmol) was added via syringe and the reaction was stirred at room temperature overnight. The water was removed in vacuo with heating to 80° C., yielding product as a colorless liquid.

来源