反应 #955933

反应方程式

methyl 2,4-dimethylbenzoate

hydrazine

→

2,4-dimethylbenzohydrazide

溶剂

MeOH

反应条件

后处理

1. 1
   温度the mixture was heated
2. 2
   温度under reflux for 40 hours
3. 3
   其他Then the mixture was evaporated
4. 4
   其他dried under vacuum

实验过程

To a solution of methyl 2,4-dimethylbenzoate (2 g, 12.2 mmol) in MeOH (10 mL) was added anhydrous hydrazine (1.95 mL, 61 mmol) and the mixture was heated under reflux for 40 hours. Then the mixture was evaporated and dried under vacuum to give 2,4-dimethylbenzohydrazide as a white solid (2 g, 100%; MS (M+H, 165).

来源