反应 #95263

ord-1fe7c09f8c9044da82932012f238a8d7

反应方程式

CCOC(=O)CCCCCC1CCCCC1=O
2-(5-carbethoxypentyl)cyclohexan-1-one
CC(=O)OC(C)=O
acetic anhydride
→
CCOC(=O)CCCCCC1=C(OC(C)=O)CCCC1
1-acetoxy-2-(5-carbethoxypentyl)cyclohex-1-ene

反应物

CCOC(=O)CCCCCC1CCCCC1=O
2-(5-carbethoxypentyl)cyclohexan-1-one
CC(=O)OC(C)=O
acetic anhydride

试剂

无

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

Treatment of 2-(5-carbethoxypentyl)cyclohexan-1-one (Example 15) with acetic anhydride by the procedure of Example 24 is productive of the subject compound.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US04343949uspto-grants-1982_08