反应 #94713

ord-db2425f0b7f64770bfd648c6ab889872

反应方程式

C=C(C)C(=O)OCC(C)OC(=O)c1cccc(S(=O)(=O)O)c1C(=O)O
( a )
C=C(C)C(=O)OCC(C)OC(=O)c1cccc(S(=O)(=O)O)c1C(=O)O
methacryloxyisopropyl acid sulfophthalate
C=C(C)C(=O)OCCO
β-hydroxyethyl methacrylate
C=CCC1(S(=O)(=O)O)CC(=O)OC1=O
allyl-sulfo-succinic anhydride
→
C=CCC1CC(=O)OC1=O
allyl-succinic acid anhydride

反应物

C=C(C)C(=O)OCC(C)OC(=O)c1cccc(S(=O)(=O)O)c1C(=O)O
( a )
C=C(C)C(=O)OCC(C)OC(=O)c1cccc(S(=O)(=O)O)c1C(=O)O
methacryloxyisopropyl acid sulfophthalate
C=C(C)C(=O)OCCO
β-hydroxyethyl methacrylate
C=CCC1(S(=O)(=O)O)CC(=O)OC1=O
allyl-sulfo-succinic anhydride

试剂

无

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

By procedure (7) (a) above, β-hydroxyethyl methacrylate is esterified with an equimolar amount of allyl-sulfo-succinic anhydride obtained by the sulfonation of allyl-succinic acid anhydride obtained from propene and maleic anhydride by a procedure analogous to that of (8) (b) hereinabove.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US04131736uspto-grants-1978_12