反应 #939017

反应方程式

mono-perphthalic acid

mono-perphthalic acid

sodium sulfite

→

2-Butylsulfonylcyclopentanone

溶剂

ether

反应条件

后处理

1. 1
   洗涤the resultant solution was washed
2. 2
   其他evaporated
3. 3
   其他to remove the solvent
4. 4
   workup.DISTILLATIONdistilled

实验过程

2-Buthylthiocyclopentanone (88 g) was reacted with a 30% excess solution of mono-perphthalic acid in ether at 0° C. After the reaction was completed, the excess mono-perphthalic acid was treated with sodium sulfite, and the resultant solution was washed, evaporated to remove the solvent, and then distilled, thereby giving 2-butylsulfonylcyclopentanone (78 g).

来源