反应 #9346

反应方程式

Sodium propanoate

2,6-dipropylphenol

→

phenol

2,6-dipropyl-4-propionylphenol

溶剂

Triflic Acid

反应条件

后处理

1. 1
   其他The resulting waxy solid was purified by chromatography on silica gel

实验过程

Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol.

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