反应 #927262

反应方程式

8-bromooct-1-ene

sodium iodide

→

8-iodooct-1-ene

收率 91.4%

溶剂

acetone

acetone

反应条件

后处理

1. 1
   其他8-Iodooct-1-ene was prepared
2. 2
   其他the residue was partitioned between water and ether
3. 3
   洗涤The aqueous phase was washed with brine
4. 4
   干燥dried over magnesium sulfate

实验过程

8-Iodooct-1-ene was prepared by refluxing 5 g of 8-bromooct-1-ene (26 mmol) and 10 g of sodium iodide in 50 ml of acetone for 1 hour. The acetone was stripped and the residue was partitioned between water and ether. The aqueous phase was washed with brine, dried over magnesium sulfate and stripped to give 5.66 g of 8-iodooct-1-ene.

来源