反应 #848

反应方程式

p-hydroxybenzoic acid

decanoic acid chloride

pyridine

→

p-decanoyloxybenzoic acid

溶剂

water

反应条件

后处理

1. 1
   萃取an organic layer was extracted with dichloromethane
2. 2
   洗涤The organic layer was washed with 1N hydrochloric acid
3. 3
   干燥dried over anhydrous sodium sulfate
4. 4
   workup.DISTILLATIONthe solvent was distilled off
5. 5
   洗涤residue was washed with n-hexane
6. 6
   其他dried
7. 7
   其他to give a crude end product

实验过程

10 Grams of p-hydroxybenzoic acid and 15 g of decanoic acid chloride were stirred at room temperature, and 7.2 g of pyridine was dropwise added. After the mixture was stirred for 1 day, a reaction product was poured into water, and an organic layer was extracted with dichloromethane. The organic layer was washed with 1N hydrochloric acid and dried over anhydrous sodium sulfate, the solvent was distilled off, and then residue was washed with n-hexane and then dried to give a crude end product.

来源