反应 #84025

反应方程式

Oxalyl chloride

t-butyl alcohol

→

Compound 34

Chloro-Oxo-Acetic Acid t-Butyl Ester

溶剂

ether

反应条件

后处理

1. 1
   其他The solvent was evaporated under vacuum

实验过程

Oxalyl chloride (232 μL, 2.8 mmol) and t-butyl alcohol (228 μL) were combined in ether (6.7 mL) under nitrogen at 0° C. The resulting mixture was stirred for 30 minutes at room temperature. The solvent was evaporated under vacuum to form Compound 34.

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