反应 #8315

ord-a73591ed459f4fe0b68338a627538e04

反应条件

温度
80°CELSIUS
详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他The thionyl chloride is evaporated

实验过程

A mixture of 3-benzyl-4-bromo-butyric acid (2.0 g, 7.78 mmol) and thionyl chloride (6.0 mmol) is heated to 80° C. for 2 h. The thionyl chloride is evaporated to yield 3-benzyl-4-bromo-butyryl chloride 2.1 g (99%), as a colorless liquid.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07087626B2uspto-grants-2006_08