反应 #8315
ord-a73591ed459f4fe0b68338a627538e04
反应条件
温度
80°CELSIUS
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他The thionyl chloride is evaporated
实验过程
A mixture of 3-benzyl-4-bromo-butyric acid (2.0 g, 7.78 mmol) and thionyl chloride (6.0 mmol) is heated to 80° C. for 2 h. The thionyl chloride is evaporated to yield 3-benzyl-4-bromo-butyryl chloride 2.1 g (99%), as a colorless liquid.