反应 #830121

ord-a320a7be91fc48da83367697205db439

反应方程式

O=C([O-])[O-].[Ca+2]
calcium carbonate
OC[C@@H](O)[C@H](O)[C@@H](O)CO
xylitol
OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)CO
sorbitol
收率 22.0%

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    workup.ADDITIONTo this mixture was added 0.45 grams of F, D and C Blue No
  2. 2
    温度was heated separately

实验过程

A stabilized, substantially non-volatile mixture of 15 grams of a medium chain triglyceride and 22.5 grams of menthol crystals was formed. To this mixture was added 0.45 grams of F, D and C Blue No. 1 H.T. Lake. A second mixture comprising 22.5 grams of polyethylene glycol (8,000 carbowax) with 12 grams of hydrogenated cottonseed oil was heated separately. An additional mixture of 129.6 grams of corn sugar solids (maltodextrose M-365), 45 grams of hydroxypropylmethyl cellulose, 1.5 grams of lecithin, 15 grams of calcium carbonate, 0.4 grams of capsicum, 30 grams of xylitol and 6 grams of sorbitol was formed. The separate mixtures were then combined and placed in a spinning machine having a 7" cable heater head with a 0.030" gap between heating cables. The mixture was then flash flowed to produce a delivery system containing menthol flavor crystals.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05556652uspto-grants-1996_09