反应 #828712

反应方程式

9-borabicyclo[3.3.1]nonane

HCl

→

title compound

收率 75.0%

B-chloro-9-borabicyclo[3.3.1]nonane

收率 75.0%

溶剂

hexane

ether

反应条件

实验过程

The title compound was prepared in 75% yield following the method of Example 1 by treating 9-borabicyclo[3.3.1]nonane (9-BBN, Aldrich Chemical Company, Inc., Milwaukee, Wis.) with anhydrous HCl in ether. 11B NMR δ 79 ppm in hexane, bp 65° C. (0.3 mm).

来源