反应 #82144
ord-165c21acb8a34d9c9681683a969f54e5
试剂
无
溶剂
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1过滤The polymer was filtered
- 2萃取The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor
- 3其他dried
- 4其他to afford a pale brown solid which
实验过程
The resulting heterogeneous reaction mixture, which was lumpy and hardened, was neutralized by addition of 15% aqueous tartaric acid solution. The polymer was filtered and a small portion was ground thoroughly. The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor and dried to afford a pale brown solid which was not soluble to any extent in distilled water.