反应 #806269

反应方程式

triethylammonium 2-(6-cyano-1-hexyn-1-yl)adenosine 5′-monophosphate

HCl

→

2-(6-cyano-1-hexyn-1-yl)adenosine 5′-monophosphate

溶剂

water

water

反应条件

后处理

1. 1
   workup.ADDITIONwas added
2. 2
   过滤the resultant mixture was filtered
3. 3
   洗涤The residue was washed with water (20 mL)

实验过程

A triethylammonium 2-(6-cyano-1-hexyn-1-yl)adenosine 5′-monophosphate (1.1 g) was dissolved in water (20 mL), and, under ice-cooling conditions, 1N HCl solution (2 mL) was added thereto, followed by standing for 10 minutes. After having been diluted with water (20 mL), the resultant mixture was filtered. The residue was washed with water (20 mL) and then with ethanol (20 mL×2), to thereby yield 617 mg of the above-titled compound as a colorless amorphous substance.

来源