反应 #806262
ord-fc90dcaa79f548298fe76ba67b91ec5b
反应方程式
2,2,4-trimethylpentan-1,3-diol
prenyl chloride
→
1-(3-methyl-2-butenyloxy)-2,2,4-trimethylpentan-3-ol
收率 92.0%
反应条件
详细条件
See reaction.notes.procedure_details.
实验过程
Treatment of 2,2,4-trimethylpentan-1,3-diol with prenyl chloride employing the alkylation reaction conditions described above provided 1-(3-methyl-2-butenyloxy)-2,2,4-trimethylpentan-3-ol in 92.0% yield (393.8 g, b.p.=82–84 C./0.8 mmHg).