反应 #806243

ord-1692dc1ed806452ca7382107d965b1e2

反应方程式

Oc1ccccc1
phenol
O=S(=O)(O)O
sulfuric acid
O=S(=O)(O)O
sulfuric acid
O=S(=O)(O)O
sulfuric acid
Oc1ccccc1
Phenol
Oc1ccccc1
phenol
Oc1ccccc1
phenol
Oc1ccccc1
Phenol
O=S(=O)(O)c1ccc(O)cc1
phenolsulfonic acid

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他A facial exfoliant was prepared

实验过程

A facial exfoliant was prepared. A solution of phenolsulfonic acid was prepared as described in Example 1, except that the weight of available stock liquefied phenol USP was calculated and prepared for 4.0 moles of phenol. The amount of available stock sulfuric acid NF that contained 4.0 moles was calculated. The weight of sulfuric acid NF was 392.32 grams. The 4.0 moles of sulfuric acid NF was treated as described in Example 1. A quantity of 400 mL of Liquified Phenol USP was added to a 600 mL beaker. A quantity of 4.0 moles of phenol as Liquefied Phenol USP was added to a 1 L Corning Pyrex No. 1395 bottle using the Mettler PS-5002-S balance.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07132111B2uspto-grants-2006_11