反应 #74712

ord-01bd8ea14e7b4957854705e522f04f34

反应方程式

Sc1ccccc1
thiophenol
O=C(O)CNC(=O)OCc1ccccc1
Z-Gly
O=C(CNC(=O)OCc1ccccc1)OSc1ccccc1
N-benzyloxycarbonyl-glycine-phenythio ester
收率 62.0%

试剂

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

Using thiophenol and Z-Gly.OH, Example 78 was repeated; except that dichloromethane was used in place of ethyl acetate as the extraction solvent, to obtain N-benzyloxycarbonyl-glycine-phenythio ester (hereinafter represented by ##STR12## in a yield of 62%.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US04173563uspto-grants-1979_11