反应 #742269

ord-9f5289c08f2941199dbef871e4dcb7eb

反应方程式

CCN(C)CC
diethylmethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(C)CC
diethylmethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
→
CC[NH+](C)CC.O=S(=O)([O-])C(F)(F)F
Diethylmethylammonium Trifluoromethanesulfonate

反应物

CCN(C)CC
diethylmethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(C)CC
diethylmethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid

试剂

无

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    温度while being cooled by liquid nitrogen
  2. 2
    其他thus obtaining a target ionic conductor

实验过程

Equimolar amounts of diethylmethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed diethylmethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US08071253B2uspto-grants-2011_12