反应 #725866

ord-735f1f581498461dbdaff74b2d3091a4

反应方程式

O.O.O.O.O.O.O.O.O.O=[N+]([O-])[O-].O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Al+3]
aluminum nitrate nonahydrate
→
O=[N+]([O-])[O-].O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Al+3]
aluminum nitrate

反应物

O.O.O.O.O.O.O.O.O.O=[N+]([O-])[O-].O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Al+3]
aluminum nitrate nonahydrate

试剂

无

溶剂

O
water

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

375.13 g (1 mole) of aluminum nitrate nonahydrate (Al(NO3)3.9H2O)(manufactured by Kansai Catalyst Co., Ltd., reagent grade, appearance: powder) was dissolved in water to obtain 1000 cm3 of an aluminum nitrate solution. 100 cm3 of the aluminum nitrate solution was added with 2.83 g of seed crystal described above (0.566 g in terms of Al2O3) to obtain a mixture. Then water was evaporated from the mixture under conditions of 75° C. by using a pressure-reduced drier, to obtain a powder. The amount of the seed crystal in terms of Al2O3 was 10 parts by weight per 100 parts by weight of the powder.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07691362B2uspto-grants-2010_04