反应 #68451

ord-f0f27b3d5f4445b495693b4ff407852b

反应方程式

CC(C)(C)CC(C)(C)c1ccc(O)c(-n2nc3ccccc3n2)c1
Cyasorb 5411
C=C(C)C(=O)OC
PMMA
C=C(C)C(=O)OC
PMMA
COCC(C)O
1-methoxy-2-propanol
CC(=O)CC(C)(C)O
diacetone alcohol
CCCCCCCCOC(=O)CCc1cc(-n2nc3ccccc3n2)c(O)c(C(C)(C)C)c1
Tinuvin 384
CCC(C)(C)c1cc(-n2nc3ccccc3n2)c(O)c(C(C)(C)CC)c1
Tinuvin 328
CC(C)(C)CC(C)(C)c1ccc(O)c(-n2nc3ccccc3n2)c1
Cyasorb 5411
CCCCCCCCOC(=O)CCc1cc(-n2nc3ccccc3n2)c(O)c(C(C)(C)C)c1
Tinuvin 384
CCC(C)(C)c1cc(-n2nc3ccccc3n2)c(O)c(C(C)(C)CC)c1
Tinuvin 328
c1ccc2[nH]nnc2c1
Benzotriazole

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他A coating solution was prepared
  2. 2
    workup.WAITthe coated film was baked for 1 hour at 100° C

实验过程

A coating solution was prepared containing 7 grams (g) of Elvacite 2041 PMMA, 79 g of 1-methoxy-2-propanol, 14 g of diacetone alcohol, 0.85 g of Tinuvin 384, 0.43 g of Tinuvin 328, 0.22 g of Cyasorb 5411, and 2 drops of BYK 331 surfactant. Thus, the solution contains 7% PMMA by total weight and 10% Tinuvin 384, 5% Tinuvin 328, and 2.5% Cyasorb 5411 based on solids. This solution was applied by flow coating onto 7 mil (177.8 μm) polycarbonate films 10 inches (25.4 cm) wide and 15 inches (38.1 cm) long, the solvent was flashed at 50° C. for 10 minutes, and the coated film was baked for 1 hour at 100° C. The top 5 inches (12.7 cm) of the films was discarded.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US08525191B2uspto-grants-2013_09