反应 #67855

反应方程式

3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid

intermediate 2

3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid

O-methyl-hydroxylamine

→

N-Benzyloxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide

反应条件

后处理

1. 1
   其他LC/MS [10.01 min; 480 (M+1)]

实验过程

N-Benzyloxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.25 mmol of 3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid (intermediate 2) and 0.36 mmol of O-methyl-hydroxylamine. LC/MS [10.01 min; 480 (M+1)]

来源