反应 #676209

反应方程式

Bromine

1-(1,3-thiazol-2-yl)ethanone

→

2-bromo-1-(1,3-thiazol-2-yl)ethanone

收率 100.0%

溶剂

AcOH

反应条件

后处理

1. 1
   浓缩was concentrated under reduced pressure

实验过程

Bromine (70 μL, 1 mmol) was added to a mixture of 1-(1,3-thiazol-2-yl)ethanone (200 mg, 2 mmol) in AcOH (5 mL). The reaction mixture was stirred at 100° C. for 30 min. and was concentrated under reduced pressure to give 2-bromo-1-(1,3-thiazol-2-yl)ethanone as an oil (100%) used as crude.

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