反应 #674286

反应方程式

calcium chloride

hydrogen phosphate

NaOH

→

Calcium Phosphate

反应条件

后处理

1. 1
   其他CaP NPs
2. 2
   其他were obtained by filtration of the suspension through a 0.22 μm
3. 3
   过滤filter
4. 4
   其他CaP NPs
5. 5
   其他were stored at 4° C. before use
6. 6
   其他CaP/ZOL-NPs complexes (CaPZ NPs) were prepared
7. 7
   workup.ADDITIONby mixing a CaP NPs dispersion with an aqueous solution of ZOL
8. 8
   浓缩at different ZOL concentrations (10 mg/ml of ZOL in water or 50 mg/ml of ZOL in phosphate buffer at pH 9.5)

实验过程

An aqueous solution of calcium chloride (18 mM) was added, dropwise and under magnetic stirring, to an aqueous solution on dibasic hydrogen phosphate (10.8 mM). The pH of both solutions was adjusted beforehand to 9.5 with NaOH. CaP NPs were obtained by filtration of the suspension through a 0.22 μm filter. CaP NPs were stored at 4° C. before use. CaP/ZOL-NPs complexes (CaPZ NPs) were prepared by mixing a CaP NPs dispersion with an aqueous solution of ZOL at different ZOL concentrations (10 mg/ml of ZOL in water or 50 mg/ml of ZOL in phosphate buffer at pH 9.5), at a volume ratio of 50:1.

来源