反应 #6698

反应方程式

7-chlorolepidine

CH3I

diethyl ether

→

7-chloro-1-methyllepidinium iodide

溶剂

CH3CN

反应条件

后处理

1. 1
   温度at reflux for two hours
2. 2
   其他to give a yellow powder

实验过程

A portion of the 7-chlorolepidine (80 mg) prepared as above was methylated by heating with CH3I (0.5 ml) in CH3CN (1 ml) at reflux for two hours. The mixture was treated with diethyl ether, followed by centrifugation, to give a yellow powder.

来源