反应 #6683

反应方程式

[R]-1-trifluoromethylheptyl 4-benzyloxybenzoate

→

[R]-1-Trifluoromethylheptyl 4-hydroxybenzoate

收率 99.0%

溶剂

ethyl acetate

反应条件

后处理

1. 1
   过滤Then the catalyst was filtered out
2. 2
   其他filtrate was evaporated to dryness
3. 3
   其他to give the pure compound in yield of 99%

实验过程

2.2 g of [R]-1-trifluoromethylheptyl 4-benzyloxybenzoate, (13) 100 mg of PdOH/C in 50 ml of ethyl acetate was stirred at RT over night under H2 atmosphere. Then the catalyst was filtered out and filtrate was evaporated to dryness to give the pure compound in yield of 99%.

来源