反应 #66010

反应方程式

allyl bromide

diethylene glycol

→

Diethylene glycol monoallyl ether

收率 82.0%

溶剂

THF NaH

反应条件

后处理

1. 1
   其他The product was obtained in 82% yield
2. 2
   workup.DISTILLATIONafter distillation

实验过程

Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.

来源