反应 #651855

ord-cd73f84037244cc6a695c8ccf5276666

反应方程式

CCCCCCCCc1ccc2c(c1)CC(F)c1cc(CCCCCCCC)ccc1-2
9-fluoro-2,7-dioctyl-9,10-dihydrophenanthrene
N#CC1=C(C#N)C(=O)C(Cl)=C(Cl)C1=O
DDQ
→
CCCCCCCCc1ccc2c(c1)cc(F)c1cc(CCCCCCCC)ccc12
9-Fluoro-2,7-dioctylphenanthrene

反应物

CCCCCCCCc1ccc2c(c1)CC(F)c1cc(CCCCCCCC)ccc1-2
9-fluoro-2,7-dioctyl-9,10-dihydrophenanthrene
N#CC1=C(C#N)C(=O)C(Cl)=C(Cl)C1=O
DDQ

试剂

无

溶剂

Cc1ccccc1
toluene

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

From 9-fluoro-2,7-dioctyl-9,10-dihydrophenanthrene by dehydrogenation with DDQ in toluene.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US06168838Auspto-grants-2001_01