反应 #651850

反应方程式

phenyl hydrazine

chalcone

→

chalcone hydrazone

收率 125.2%

溶剂

ethanol

反应条件

后处理

1. 1
   其他prepared
2. 2
   其他To a 500 ml round bottom flask, fitted with a magnetic stirrer
3. 3
   温度The reaction mixture refluxed overnight
4. 4
   其他A white precipitate formed
5. 5
   过滤was filtered
6. 6
   其他to yield a white solid which
7. 7
   洗涤was washed with cold ether

实验过程

Another colorant stabilizer of the present invention is a basic fuschin hydrazone, prepared as follows. To a 500 ml round bottom flask, fitted with a magnetic stirrer and a heating mantle, was placed 50 g (0.46 mole) phenyl hydrazine (Aldrich), 96.3 g (0.46 mole) chalcone (Aldrich), and 300 ml. of anhydrous ethanol. The reaction mixture refluxed overnight and then cooled to room temperature. A white precipitate formed and was filtered to yield a white solid which was washed with cold ether. 128 g (93%) chalcone hydrazone was obtained. This reaction is shown below.

来源