反应 #640566

ord-72fe3b30ad0a48d78bceee8a6f63a51b

反应方程式

Cc1ccc(S(=O)c2ccc(C)cc2)cc1
bis(4-methylphenyl)sulfoxide
Cc1ccc(Cl)cc1
4-chlorotoluene
Cc1ccc([S+](c2ccc(C)cc2)c2ccc(C)cc2)cc1.[Cl-]
tris(4-methylphenyl)sulfonium chloride

溶剂

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他The target compound was obtained
  2. 2
    其他the procedure of Synthesis Example 1 aside
  3. 3
    其他in Synthesis Example 1
  4. 4
    萃取for extraction

实验过程

The target compound was obtained by following the procedure of Synthesis Example 1 aside from using bis(4-methylphenyl)sulfoxide instead of the diphenyl sulfoxide and 4-chlorotoluene instead of the chlorobenzene in Synthesis Example 1, and increasing the amount of water for extraction.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US08048610B2uspto-grants-2011_11