反应 #640563

反应方程式

2-aminophenylboronic acid

acryloyl chloride

→

2-Acrylamido-phenylboronic acid

反应条件

后处理

1. 1
   萃取The product was extracted in acetone
2. 2
   其他dried
3. 3
   其他a rotary evaporator

实验过程

2-Acrylamido-phenylboronic acid (“2-APB”) was synthesized by reacting 2-aminophenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 2-APB was confirmed using NMR. The purity was shown to be greater than 90%.

来源