反应 #640562

反应方程式

3-amino phenylboronic acid

acryloyl chloride

→

3-Acrylamido-phenylboronic acid

反应条件

后处理

1. 1
   萃取The product was extracted in acetone
2. 2
   其他dried
3. 3
   其他a rotary evaporator

实验过程

3-Acrylamido-phenylboronic acid (“3-APB”) was synthesized by reacting 3-amino phenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 3-APB was confirmed using NMR. The purity was about 90%, TLC showing very little contamination.

来源