反应 #63786

ord-c6297e97bed54076a52d42942f386a2e

溶剂

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他was kept at 40° C.
  2. 2
    其他removed from the resulting emulsion by pH-adjustment

实验过程

In 3,000 ml of water were dissolved 28 g of gelatin and 13.2 g of benzotriazole, and the solution was kept at 40° C. while stirring. To the solution was added 100 ml of an aqueous solution of 17 g of silver nitrate over 2 minutes. Excessive salts were sedimented and removed from the resulting emulsion by pH-adjustment. Thereafter, the emulsion was adjusted to pH 6.50 to obtain a silver benzotriazole emulsion. The yield of the emulsion was 400 g.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US04767690uspto-grants-1988_08