反应 #63436
ord-9b579c6ea71c44829cf397c559a47b98
反应方程式
5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile
sodium ethanethiolate
→
ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate
反应条件
详细条件
See reaction.notes.procedure_details.
实验过程
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and sodium ethanethiolate in ethanethiol there is obtained ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate and therefrom with hydrochloric acid in alcohol there is obtained the hydrochloride, m.p. 220° C. (with decomposition);