反应 #632044

反应方程式

4-fluoroindoline

D-glucose

ethyl alcohol

→

4-fluoro-1-(β-D-glucopyranosyl)indoline

溶剂

H2O

反应条件

后处理

1. 1
   温度was refluxed under argon atmosphere for 24 hours
2. 2
   其他The solvent was evaporated under reduced pressure

实验过程

A mixture of 4-fluoroindoline (185 mg) and D-glucose (267 mg) in H2O (0.74 ml)-ethyl alcohol (9 ml) was refluxed under argon atmosphere for 24 hours. The solvent was evaporated under reduced pressure to give crude 4-fluoro-1-(β-D-glucopyranosyl)indoline, which was used in the subsequent step without further purification.

来源