反应 #632031

反应方程式

isobutyric acid

tetramethylammonium hydroxide

→

title compound ( 13 )

Tetramethylammonium Isobutyrate

反应条件

后处理

1. 1
   其他The water was removed under reduced pressure
2. 2
   其他azeotroped with toluene (2×2 L)

实验过程

To a 20 L round bottom flask was added isobutyric acid (1300 mL, 14 mol), and an aqueous solution of 25% tetramethylammonium hydroxide (5 L, 14 mol). The water was removed under reduced pressure, and azeotroped with toluene (2×2 L) to leave the title compound (13) as an amber liquid, which was used without further purification.

来源