反应 #606439

反应方程式

Methacrylic anhydride

N-(2-hydroxyethyl)-N-ethylaniline

→

N-(2-acryloyloxyethyl)-N-ethylaniline

溶剂

pyridine

反应条件

后处理

1. 1
   温度On cooling the mixture

实验过程

Methacrylic anhydride (7.7 g, 0.05 mol) is added to a solution of N-(2-hydroxyethyl)-N-ethylaniline (6.6 g, 0.04 mol) in pyridine (25 ml) and the mixture is stirred at 55° C. for 2 hours. On cooling the mixture is passed through silica gel to give N-(2-acryloyloxyethyl)-N-ethylaniline as a pale yellow oil. 5.3 g, 65%

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