反应 #59908

反应方程式

( 6f )

2-(((4-((2-methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

(2,2-diethyl-1,3-dioxan-5-yl)methanol

→

title compound

收率 9.7%

2-(((4-((2,2-diethyl-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

收率 9.7%

反应条件

后处理

1. 1
   其他obtained in the step (23a)

实验过程

The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using (2,2-diethyl-1,3-dioxan-5-yl)methanol obtained in the step (23a) to obtain the title compound (164 mg, total yield: 9.7%) as a light yellow solid.

来源