反应 #595369

反应方程式

methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate

→

title compound

methyl 4-hydroxy-2-isopropylbenzoate

溶剂

methanol

反应条件

后处理

1. 1
   过滤Then the mixture was filtered
2. 2
   浓缩the filtrate was concentrated

实验过程

To a solution of methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate (i-1d) (4.6 g, 16.3 mmol) in methanol (100 ml) was added Pd/C (0.46 g). The mixture was stirred at rt under H2 atmosphere for 24 h. Then the mixture was filtered, and the filtrate was concentrated to afford the title compound. LCMS (ESI) calc'd for C11H14O3 [M+H]+: 195.1. found: 195.1.

来源