反应 #586149

反应方程式

[2-chloro-4-fluoro-5(3-trifluoromethyltriazolyl)phenyl] methyl sulfide

2-chloro-4-fluoro-5(3-trifluoromethyltriazolyl)thiophenol

→

2-chloro-4-fluoro-5-(3-trifluoromethyltriazolyl)benzene

收率 85.7%

反应条件

实验过程

2.2 g (7.1 mmol) of [2-chloro-4-fluoro-5(3-trifluoromethyltriazolyl)phenyl] methyl sulfide was converted to 2-chloro-4-fluoro-5(3-trifluoromethyltriazolyl)thiophenol in the same manner as in Reference Example 1 and then to 1.8 g of 1,1′-thiodi-[2-chloro-4-fluoro-5-(3-trifluoromethyltriazolyl)benzene (yield 85.7%) in the same manner as in Reference Example 5 (1), which was used in Example 2 (4) as the starting material.

来源