反应 #577229

反应方程式

thioanisole

dimethyl sulfate

water

→

Dimethylphenylsulfonium Hydrogen Sulfate

溶剂

diethyl ether

反应条件

后处理

1. 1
   其他separated into two layers

实验过程

6.2 g (0.05 mole) of thioanisole and 6.9 g (0.055 mole) of dimethyl sulfate were stirred for 12 hours at room temperature. 100 g of water and 50 ml of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, dimethylphenylsulfonium hydrogen sulfate.

来源