反应 #577228

反应方程式

phenacyl bromide

tetrahydrothiophene

water

diethyl ether

→

Phenacyltetrahydrothiophenium Bromide

溶剂

nitromethane

反应条件

后处理

1. 1
   其他separated into two layers

实验过程

88.2 g (0.44 mole) of phenacyl bromide and 39.1 g (0.44 mole) of tetrahydrothiophene were dissolved in 220 g of nitromethane, which was stirred for 4 hours at room temperature. 800 g of water and 400 g of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, phenacyltetrahydrothiophenium bromide.

来源