反应 #5724

反应方程式

Farnesol

→

3,7,11-trimethyldodecanol

收率 94.9%

溶剂

ethanol

反应条件

后处理

1. 1
   其他After the completion of the reaction, insoluble material
2. 2
   其他was removed by filtration through a Celite layer
3. 3
   浓缩the filtrate was concentrated under reduced pressure

实验过程

Farnesol (200 g) was dissolved in ethanol (1000 ml), added with platinum oxide (1 g) and stirred for 24 hours at room temperature under hydrogen atmosphere. After the completion of the reaction, insoluble material was removed by filtration through a Celite layer and the filtrate was concentrated under reduced pressure to obtain 3,7,11-trimethyldodecanol (195 g).

来源