反应 #56148

ord-4f2e74cf7f7a47359f143a62f1a59dc4

反应方程式

COc1cc(C)c(C=CC(C)=CC=CC(C)=CC(=O)Cl)c(C)c1C
9-(4-methoxy-2,3,6-trimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid chloride
CC(C)N
isopropyl amine
→
COc1cc(C)c(C=CC(C)=CC=CC(C)=CC(=O)NC(C)C)c(C)c1C
9-(4-methoxy-2,3,6-trimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid isopropyl amide

反应物

COc1cc(C)c(C=CC(C)=CC=CC(C)=CC(=O)Cl)c(C)c1C
9-(4-methoxy-2,3,6-trimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid chloride
CC(C)N
isopropyl amine

试剂

无

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

9-(4-methoxy-2,3,6-trimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid chloride is reacted with isopropyl amine to produce 9-(4-methoxy-2,3,6-trimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid isopropyl amide, m.p. 200° C.;

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US04224244uspto-grants-1980_09