反应 #56147

ord-917e2d004b594ae6b9220c8c3ea5080b

反应方程式

COc1cc(C)c(C=CC(C)=CC=CC(C)=CC(=O)Cl)c(C)c1C
9-(4-methoxy-2,3,6-trimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid chloride
CN
methyl-amine
→
CNC(=O)C=C(C)C=CC=C(C)C=Cc1c(C)cc(OC)c(C)c1C
9-(4-methoxy-2,3,6-trimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid methyl amide

反应物

COc1cc(C)c(C=CC(C)=CC=CC(C)=CC(=O)Cl)c(C)c1C
9-(4-methoxy-2,3,6-trimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid chloride
CN
methyl-amine

试剂

无

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

9-(4-methoxy-2,3,6-trimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid chloride is reacted with methyl-amine to produce 9-(4-methoxy-2,3,6-trimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid methyl amide, m.p. 206° C.;

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US04224244uspto-grants-1980_09