反应 #55185

反应方程式

thionyl chloride

3-(2',4'-difluoro-4-biphenylyl)butyric acid

→

3-(2',4'-difluoro-4-biphenylyl)butyryl chloride

溶剂

benzene

反应条件

后处理

1. 1
   其他the mixture is evaporated under reduced pressure

实验过程

6 g. of thionyl chloride and 10 g. of 3-(2',4'-difluoro-4-biphenylyl)butyric acid in 80 ml. of benzene are allowed to stand at 25° for 24 hours and the mixture is evaporated under reduced pressure to give 3-(2',4'-difluoro-4-biphenylyl)butyryl chloride.

来源