反应 #54666

反应方程式

p-menth-3-oyl chloride

glycine propyl ester hydrochloride

sodium bicarbonate

→

N-p-Menth-3-oylglycine n-propyl ester

反应条件

后处理

1. 1
   workup.DISTILLATIONThe crude product was distilled b.p. 170°/0.1 mm
2. 2
   workup.DISTILLATION(After distillation the product

实验过程

Following the procedure of Example 2 p-menth-3-oyl chloride (2.0 g., 0.01 moles), was reacted with glycine propyl ester hydrochloride (1.5 g., 0.01 moles) and sodium bicarbonate (1.6 g., 0.02 moles). The crude product was distilled b.p. 170°/0.1 mm. (After distillation the product rapidly solidifies). (Found, C: 68.2; H: 1016; N: 5.0. C16H29NO3 requires, C: 67.8; H: 10.6; N: 4.9.)

来源